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Sophisticated Analytical Instrument Facility, CDRI, Lucknow

 

Sl.
No.

Instrument

Make/
Model

Major Specifications/
Accessories available

Type of measurement/analysis available

1.

 

UV-VIS Spectrometer

Perkin Elmer Lambda 15

Range: 200-850 nm

Usual analysis/studies in the region.

2.

 

FT-IR Spectrometer

Shimadzu
8201 PC

Range: 400-4000 cm-1;
Resolution: 1 cm-1

IR Spectra of liquid/solid samples, derivative.

3.

FT-IR Spectrometer

Perkin Elmer
Spectrum RX1

Range: 450-4000 cm-1;
Resolution: 1 cm-1

IR Spectra of liquid/solid samples.

4.

Polarimeter

Rudolf Autopol III

Single wavelength-589 nm; 1.5/7.5/10.0 ml cells available

   Analysis of optically active chemicals.
 

5.

FT-IR Spectrometer

Range: 50-4000 cm-1

Under procurement

6.

FT-NMR Spectrometer

Bruker Avance DRX 300

Operating frequency:
300 MHz;
Narrow bore;
Variable temperature
(-900 C to +800 C) accessory; 
Gradient accessory

1D Spectra – normal for 1H, 13C, 31P & 19F, Multinuclear in inverse mode;
2D spectroscopy (Homonuclear J correlation  COSY, COSY DQF etc., Dipolar correlation NOESY & ROESY);
Inverse spectroscopy-HMQC, HSQC, HMBC etc.; Gradient accelerated
spectroscopy; Diffusion ordered spectroscopy (DOSY); Editing
spectroscopy DEPT, INEPT;
Variable temperature studies.

7.

 

 

FT-NMR Spectrometer

Bruker Advance 400

Operating frequency: 400 MHz; 5 mm multinuclear inverse probe head, low
and high temperature facility (-90 to +800 C) and HRMAS accessory. Gel NMR measurement as well as resin bound molecules NMR measurement can be carried out.

1D Spectra – Normal for 1H, 13C, 31P,
Multinuclear in inverse mode; 2D Spectroscopy (Gradient homonuclear correlation COSY, COSYDQP etc.), Dipolar correlation NOESY & ROESY; Gradient inverse spectroscopy- Adiabatic HSQC, HMBC with double low pass filter etc.  Diffusion ordered spectroscopy; Editing spectroscopy DEPT, INEPT, Variable temperature studies.

8.

Mass Spectrometer

Jeol SX 102

Mass range: upto 2500 Da;
Resolution: upto 10,000

FAB, MIKE, CID MIKE, Linked scan; Analysis of organic and organometallic compounds.

9.

Mass Spectrometer

Shimadzu
QP 2000

Mass range: upto 900 Da;
Unit mass resolution; 
GC

 EI, GC-MS.

10.

Mass Spectrometer

Micromass
Quattro II

Mass range: upto 4000  Da;
Unit mass resolution; 
HPLC

ESI, APCI, LC-MS, MS/MS;
Capability to ionize molecules upto 100 kDa (proteins and other biomolecules);  Analysis of organic as well as organometallic compounds.

11.

Mass Spectrometer

Micromass
Tof Spec 2E

Mass range: upto 300 kDa;
Nitrogen laser- 337 nm

MALDI TOF MS; Capability to ionize molecules upto 100 kDa (peptides, proteins, other biomolecules and polymers).
 

12.

Scanning Electron Microscope

FEI Philips
XL 30

SE detector; GSED detector

3D imaging of biological specimens only.

13.

Transmission Electron Microscope

FEI Philips
Tecnai 12

CCD camera; SYS software for online measurement; Cryo Gatan stage; EDAX 

High resolution imaging of biological samples only; Immuno electron microscopy.

14.

GLC

Perkin Elmer Autosystem XL

Sample requirement: 2-5 mg

Nature of compound, solubility, melting point/boiling point, column (if known).

15.

CHNSO Elemental Analyzer

Elementar
Vario EL III

Accuracy: + 5%

C, H, N, S, O estimation of solid and liquid samples.

16.

 

CHN Elemental Analyser

Carlo Erba 1108

Accuracy: + 5%

C, H, N estimations of solid and liquid samples.

17.

Liquid Nitrogen Plant

Philips MNP 9/01

9 lts./hr.

Liquid nitrogen for R&D work.