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Sophisticated Analytical Instrument Facility, IIT-Bombay, Mumbai

 

Sl.
No.
Instrument Make/Model Major  Specifications/
Accessories available
Type of measurement/analysis available
1. FT- IR Spectrometer Nicolet 
Magna 550
 
Range: 400-4000 Cm-1  
& 50 to 600 Cm-1;
Resolution: 0.5 Cm-1 ;
Grazing/variable angle
specular reflectance; Variable angle ATR attachments.
Analysis of organic and inorganic compounds, Polymer coatings, Semi-conductors, Surface analysis and Surface orientation of molecular species.
    Nicolet 170 SX Range: 400-4000 Cm-1
Resolution: 0.06 Cm-1
 
2. ICP-Atomic Emission Spectrometer Plasma Lab Labtam 8440 Range: 160 to 800 nm, covering all important elements;
Detection limit: 0.01 to 0.1 ppm;
Hydride generator for elements like As, Sb, Sn, Hg, Se & Bi.
Analysis of elements in soil, rock, plants, effluents, water, chemicals, environmental, metallurgical, biological/clinical and pharmaceutical samples.
3. ICP-Atomic Emission Spectrometer Jobin Yuon Ultima 2 Range: 120 to 800 nm;
Detection limit: 10ppb
 
4. Fluorescence
Spectrometer
Applied Photophysics
SP-70
Excitation with nanosecond flashlamp system; Lifetime measurements down to 0.5 nanosecond; Low temperature accessory. Fluorescence studies/measurements of species in biological systems, polymers, membranes, liquid crystals, low dimensional structures, semiconductors etc.  in areas of Photobiology, Photochemistry and Photophysics.
 
5. Laser Raman Spectrometer Jobin Yvon
Ramanor
HG 2S
Range: 50 to 4000 Cm-1; 488 & 514 nm excitations; High temperature and sample spinning accessories. Analysis of powder, single crystals, liquids, thin films, polymers etc.
6. FT-NMR Spectrometer Varian
Mercury Plus 300
300 MHz machine with 5 mm probe; capable of liquid and solid sample analysis for nuclei from nitrogen to phosphorus including proton and fluorine; solid state NMR 7 mm rotor for 15N to 31P analysis. Organic, Organometallic, pharmaceutical and polymer sample analysis for structure elucidation & quality control.
7. ESR  Spectrometer Varian E-112 X-band operation 
9-10 GHz; Variable temperature & aqueous solution accessories; Goniometer/sample rotator.
ESR studies/analysis of  metals, alloys, liquid crystals, catalysts, drugs, enzymes,
proteins, gases, organic & inorganic radicals.
8. X-Ray Fluorescence   Spectrometer Philips PW2404 4 KW high power
X-Ray spectrometer;  Sample preparation accessories:  Minipress, Fusion bead machine & Powdering machine.
Analysis of liquid, solid, and power samples including  ash, soil, rock etc.  for elements  from Boron to U235.
9. GC-LC- Mass  Spectrometer Hewlett Packard 5989B Range: upto 2000 amu;
GC, HPLC, EI, CI, ES-API.
Analysis of organic compounds, bio-samples like proteins-21; GC-MS (EI, CI), DIP-MS (EI, CI), ES-MS (Softionisation).
10. CHNSO Elemental Analyzer Thermo Finnigan  FLASH EA 1112 Series Volatile liquid and solid preparation accessory Estimation of C,H,N,S,O in percentage.
11. Scanning Electron Microscope Cameca
SU-SEM probe
Resolution: upto 400 A
Magnification:
upto 40,000 x;
Accelerating Voltage:
upto 30 kV;
Fully integrated EDS/WDS system.
To study surface topography, crystallography, magnetic/electric character, composition etc. of samples in physical, minerological and biological sciences.
12. Transmission Electron Microscope Philips
CM-200
Accelerating Voltage: upto 200 kV;
Spot resolution: 2.3 0A
EDX, STEM, Local orientation measurement package (TSL-ACT), External CCD.
Study of ultrastructures of materials; Local orientation measurements in nanograms.
13. Image Analysing System Leitz
TAS PLUS
Soft imaging system;
High resolution CCD Camera, compatible high resolution frame grabber card; Image analysis software.
Classification of grain structure and inclusion analysis in metals and alloys; Size distribution analysis of powder, counting dark blemishes & holes;  Evaluating porosity of paper filters etc.
14. Thermal Analysis System (DSC/DTA/TGA) Dupont,
USA 990
TGA/DTA: Range-
Room temp. to 10000 C;
DSC: Range-
Room temp. to 6000 C.
Thermal analysis studies including transition temperatures,  Exothermic/Evelothermic heat flow measurements,  peak temperature etc.
15. Thermal Analysis System (DTA/TGA) Perkin Elmer Diamond TG/DTA Temp. range: RT to 15000 C;
Heating rate: 0.01 to
1000 C
Simultaneous DTA/TGA thermal analysis studies including transition temperatures, Exothermic/Evelothermic heat flow measurements, peak temperature etc.
16. Molecular Graphics Workstation Silicon Graphics Power Indigo 2XZ Molecular Modeling Program; BIOSYM- Insight II and Discover Softwares; TRIPOS – Alchemy III, Chemprint, Power Search Softwares. Insight II program helps to build and manipulate virtually any class of molecule or molecular system in conjunction with molecular mechanics/dynamics program DISCOVER.